Clovidipine Butyrate on Ultisil XB-C18
System adaptive solution
Rt (min) | K’ | Area (mAU*s) | Height (mAU) | Symmetry Factor | Width (min) | Plates | Resolution | Tailing Factor |
Column | Ultisil XB-C18 4.6×250 mm, 5 μm |
Detection | 220 nm |
Temperature | 35°C |
Flow Rate | 1.2 ml/min |
Injection Volume | 50 µl |
Mobile Phase
A: 0.05mol/L sodium dihydrogen phosphate (Adjust pH to 4.0 with phosphoric acid)
B: Acetonitrile:Methanol=3:2
Time(min) | A% | B% |
0 | 55 | 45 |
12 | 38 | 62 |
70 | 38 | 62 |
72 | 55 | 45 |
80 | 55 | 45 |